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Thursday, July 23, 2020 | History

1 edition of MALDI-TOF Mass Spectrometry of Synthetic Polymers found in the catalog.

MALDI-TOF Mass Spectrometry of Synthetic Polymers

by Harald Pasch

  • 300 Want to read
  • 29 Currently reading

Published by Springer Berlin Heidelberg in Berlin, Heidelberg .
Written in English

    Subjects:
  • Biochemistry,
  • Analytical biochemistry,
  • Biotechnology,
  • Chemistry,
  • Polymers

  • About the Edition

    MALDI-TOF mass spectrometry is one of the latest and most fascinating new developments in the analysis of organic compounds. Originally developed for the analysis of biomolecules, it has developed into one of the most powerful techniques for the characterization of synthetic polymers. This book describes the fundamentals of the MALDI process and the technical features of MALDI-TOF instrumentation. It reviews the application of MALDI-TOF for identification, chemical and molar mass analysis of synthetic polymers. Experimental protocols for the determination of endgroups, the analysis of homo- and copolymers, and the coupling of liquid chromatography and MALDI-TOF are discussed in detail.

    Edition Notes

    Statementby Harald Pasch, Wolfgang Schrepp
    SeriesSpringer Laboratory, Springer Laboratory
    ContributionsSchrepp, Wolfgang
    Classifications
    LC ClassificationsQD380-388
    The Physical Object
    Format[electronic resource] /
    Pagination1 online resource (xviii, 299 p.)
    Number of Pages299
    ID Numbers
    Open LibraryOL27072347M
    ISBN 103642079237, 3662050463
    ISBN 109783642079238, 9783662050460
    OCLC/WorldCa851369071

    This book presents fundamentals of one of the well-recognized mass spectrometry techniques, matrix-assisted laser desorption ionization time of fl ight mass spec- trometry (MALDI-ToF-MS). The most direct way to optimize mass spectral analysis of polymers has led to exploring new matrices, solvents, and ionizing agents. Since the first reports of the application of MALDI for synthetic polymer analysis [], significant advances in sample preparation protocols and instrumentation development have been taken place.

    The final chapter provides a valuable overview of potential future trends and developments in MALDI-TOF MS and assesses the impact of the technology in Codes: SCI, MED, SCI, SCIBIC Codes: MMFM, PSG, PNFSThema notation: MKFM, MZMP, PSG, PNFSKeywords: MALDI-TOF,mass spectrometry,diagnostic laboratory. and synthetic polymers is in the ionization process. For protein/pep-tide MALDI analysis, most samples are ionized through protonation; for synthetic polymer MALDI experiments most samples are ionized by cationization. Some polymers, such as polyethylene glycols and polymethylmeth-acylate form ions with alkali metals (added to the sample or simply.

      Anal Bioanal Chem () – DOI /sz BOOKS AND SOFTWARE IN REVIEW Liang Li (Ed.): MALDI mass spectrometry for synthetic polymer analysis David M. Hercules Published online: 27 July Springer-Verlag Bibliography cited is pretty much up-to-date as of but is spotty in MALDI mass spectrometry for coverage from forward. .   Time-of-flight (TOF) mass separation [] is the technique most often applied to synthetic polymers due to their high molecular masses, typically in excess of u and often much greater (into the u range and beyond).No other mass separation technique can reach such high masses. The TOF signal, s(t i), is collected on equal intervals of time.


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MALDI-TOF Mass Spectrometry of Synthetic Polymers by Harald Pasch Download PDF EPUB FB2

MALDI-TOF Mass Spectrometry of Synthetic Polymers (Springer Laboratory) - Kindle edition by Pasch, Harald, Schrepp, Wolfgang. Download it once and read it on your Kindle device, PC, phones or tablets. Use features like bookmarks, note taking and highlighting while MALDI-TOF Mass Spectrometry of Synthetic Polymers book MALDI-TOF Mass Spectrometry of Synthetic Polymers (Springer Laboratory).4/5(1).

MALDI-TOF mass spectrometry is one of the latest and most fascinating new developments in the analysis of organic compounds.

Originally developed for the analysis of biomolecules, it has developed into one of the most powerful techniques for the characterization of synthetic by: Buy MALDI-TOF Mass Spectrometry of Synthetic Polymers (Springer Laboratory) by Pasch, Harald, Schrepp, Wolfgang (ISBN: ) from Amazon's Book Store.

Everyday low prices and free delivery on eligible orders.4/5(1). MALDI-TOF mass spectrometry is one of the latest and most fascinating new developments in the analysis of organic compounds.

Originally developed for the analysis of biomolecules, it has developed into one of the most powerful techniques for the characterization of synthetic polymers.

This bookBrand: Springer-Verlag Berlin Heidelberg. MALDI-TOF Mass Spectrometry of Synthetic Polymers by Harald Pasch,available at Book Depository with free delivery worldwide.

Desorption electrospray ionisation mass spectrometry and tandem mass spectrometry of low molecular weight synthetic polymers. Rapid Communications in Mass Spectrometry20 (18), Cited by:   Maldi Mass Spectrometry for Synthetic Polymer Analysis, Volume Editor(s): Liang Li; "Overall, I highly recommend this book for any polymer scientist with access to MALDI-MS as it will aid in the better planning of experiments and interpretation of the results.

This is definitely a book for beginning graduate students in the field and. assisted laser desorption/ionization mass spectrometry (MALDI-MS) to the analysis of synthetic polymers, and includes data obtained by Toyota CRDL.

In MALDI-MS of synthetic polymers, the selection of a matrix and cationizing agent, as well as the sample preparation techniques, are very important to obtaining a successful spectrum. MALDI-MS.

The process of MALDI-TOF mass spectrometry. Figure 3. The process of MALDI-TOF mass spectrometry (Clark A. E., et al.; ) The analyte should be soluble to at least about mg/ml in some solvent.

And the matrix is dissolved to yield either a. characterization of synthetic polymers, mass spectro-metry is of increasing importance (Smith et al., ).

In the past, mass spectrometry of synthetic polymers was hardly possible: as a rule, polymers had to be degraded thermally or chemically prior to mass spectrometric Mass Spectrometry Reviews,18, – Investigating the effect of mixing ratio on molar mass distributions of synthetic polymers determined by MALDI-TOF mass spectrometry using design of experiments.

Journal of the American Society for Mass Spectrometry21 (11), Cited by: In mass spectrometry, matrix-assisted laser desorption/ionization (MALDI) is an ionization technique that uses a laser energy absorbing matrix to create ions from large molecules with minimal fragmentation.

It has been applied to the analysis of biomolecules (biopolymers such as DNA, proteins, peptides and sugars) and large organic molecules (such as polymers, dendrimers and other.

His particular interest is focused on the application of MALDI-TOF MS of synthetic polymers by developing suitable hyphenated chromatography approaches for efficient reduction of complexity. For the last 15 years, he is chairperson of the annual German workshop on polymer analysis by MALDI-TOF mass spectrometry.

MALDI−TOF mass spectral characterization of polymers containing an azide group: evidence of metastable ions. Macromolecules. ; – [PMC free article] [Google Scholar] Zenobi R.

Ionization processes and detection in MALDI-MS of polymers. In: Li L, editor. MALDI Mass Spectrometry for Synthetic Polymer Analysis. Characterization of synthetic polymers by MALDI-MS Giorgio Montaudo a,*, Filippo Samperi b, Maurizio S. Montaudo b a Chemistry Department, University of Catania, Viale A.

Doria 6, Catania, Italy b Institute of Chemistry and Technology of Polymers, CNR, Viale A. Doria 6, Catania, Italy Received 23 June ; received in revised form 30 September ; accepted 20 December Maldi-Tof Mass Spectrometry of Synthetic : ISBN: Format Type: eBook PDF / e-Pub: Author: fearful Mirrof: Last download: Detail: Download Maldi-Tof Mass Spectrometry of Synthetic Books Do you know of any more places to download free digital books.

MALDI-TOF mass spectrometry is one of the latest and most fascinating new developments in the analysis of organic compounds. Originally developed for the analysis of biomolecules, it has developed into one of the most powerful techniques for the characterization of synthetic polymers. This book describes the fundamentals of the MALDI process and the technical features of MALDI-TOF.

In recent years, matrix assisted laser desorption/ionization time-of-flight (MALDI-TOF) mass spectroscopy has become a routine analytical tool for the structural analysis of polymers, complementing NMR and other traditional techniques, a noteworthy change with respect to the past, when mass spectrometry (MS) was seldom used.

MALDI-TOF mass spectrometry is one of the latest and most fascinating new developments in the analysis of organic compounds. It reviews the application of MALDI-TOF for identification, chemical and molar mass analysis of synthetic polymers.

Title: Current Mass Spectrometry of Synthetic Polymer VOLUME: 11 ISSUE: 10 Author(s): Meiyu He and Hui Chen Affiliation:Department of Chemistry,Peking University,Beijing, China.

Keywords:Cation Salts, post-source decay, polydimethylsiloxane, Dendrimers, liquid chromatography critical conditions Abstract: As the well-known soft ionization techniques, matrix assisted laser. Mass spectrometry (MS) is well suited for analysis of the identity and purity of synthetic peptides.

The sequence of a synthetic peptide is most often known, so the analysis is mainly used to confirm the identity and purity of the peptide.

Here, simple procedures are described for MALDI-TOF-MS and LC-MS of synthetic peptides.MALDI-TOF Mass Spectrometry of Synthetic Polymers.

By Harald Pasch (Deutsches Kunststoff-Institut, Darmstadt, Germany) and Wolfgang Schrepp (BASF AG, Ludwigshafen, Germany). Springer-Verlag: Berlin, Heidelberg, New York. xviii + pp. $ ISBN This book offers a summary of the fundamentals and the. A. Marie, F. Fournier, J.C. TabetCharacterization of synthetic polymers by MALDI-TOF/MS: Investigation into new methods of sample target preparation and consequence on mass spectrum finger print Anal.

Chem., 72 (), pp.